Three runs of six open system mesocosms run with 15N tracer addition from (oyster reef N2O emission project) | N2O and SF6 concentrations were measured on a gas chromatograph with electron capture detector (GC-ECD).
| gas chromatograph with electron capture detector (GC-ECD) |
Amino acid compound specific nitrogen isotopic analysis (AA-CSIA) data from reef fish samples collected over a 4 year period from 2008 to 2012 from the Hawaiian Islands | The d15N values of derivatized samples were determined using a Delta V Plus mass spectrometer interfaced to a Trace
GC gas chromatograph through a GC-C III combustion furnace.
| gas chromatograph |
Amino acid compound-specific isotope analysis (AA-CSIA) of tissue samples from four distinct trophic groups across the food web in the pelagic eastern tropical Pacific Ocean; samples collected on NOAA cruises from July to December 2006 | The d15N values of individual AAs were measured using an isotope ratio mass spectrometer (IRMS) (Delta PlusXP, Delta V Plus or MAT 253) interfaced with a gas chromatograph (Trace GC) through a GC-C III combustion furnace (980 degrees C), reduction furnace (650 degrees C), and liquid-N cold trap.
| gas chromatograph (Trace GC) |
Amino acid compound specific isotope analyses of abyssal deposit feeders, gut contents, and surrounding surface sediments collected on R/V Atlantis cruise AT42-10 and R/V Western Flyer Pulse 72 in the eastern North Pacific in 2019 | Nitrogen isotope composition of amino acids was determined using an isotope ratio mass spectrometer (Thermo Scientific Delta V Plus) interfaced with a Thermo Finnigan GC-C III.
| Thermo Finnigan GC-C III |
Concentrations of acrylate and dimethylsulphoniopropionate from the surface of coral reefs sampled in Moorea, French Polynesia in April 2018 | DMS was analyzed using a cryogenic purge-and-trap system and a Shimadzu GC-14A with a flame photometric detector.
| Shimadzu GC-14A |
Biological turnover of acrylate and dimethylsulphoniopropionate from coral reefs sampled in Moorea, French Polynesia in April 2018 | DMS was analyzed using a cryogenic purge-and-trap system and a Shimadzu GC-14A with a flame photometric detector
| Shimadzu GC-14A |
Amino acid d13C values of diatoms, bacteria, and core M772-003-2 samples from the R/V Meteor (M77) in the Peruvian ocean margin from November to December 2008. | Used with MAT 253 isotope ratio mass spectrometer (IRMS) via a GC-III combustion (C) interface (Thermo-Finnigan Corporation)
| Thermo Trace GOLD GC |
Amino acid d13C values of Thalassiosira weissflogii of ten different treatments; collections from R/V Meteor M77 in the Peruvian ocean margin from November to December 2008. | Used with MAT 253 isotope ratio mass spectrometer (IRMS) via a GC-III combustion (C) interface (Thermo-Finnigan Corporation)
| Thermo Trace GOLD GC |
Bulk and AA d15N values for ala, glu, and phe from phytoplantkon and grazers grown in lab chemostats | For experiments 1-4, we used a Delta V Plus mass spectrometer interfaced with a Trace GC gas chromatograph through a GC-C III combustion furnace (980C), reduction furnace (650C), and liquid nitrogen cold trap as described in Hannides et al. (2009).
For experiments 5-6 we used a Delta V Plus mass spectrometer (Thermo Scientific) interfaced through a Conflo IV to a GC 1310 gas chromatograph coupled to a GC Isolink combustion-reduction furnace (1000C) and liquid nitrogen cold trap.
| Trace GC gas chromatograph, GC 1310 gas chromatograph |
Amino acid enantiomeric ratios (D/L) of high and low molecular weight (HMW, LMW) DOM collected from the North Pacific Subtropical Gyre and Central North Atlantic | | GC-MS; Agilent 7890A + 5975B |
Amino acid isotopes from mussels along the California margin from 2009-2013 (Amino Acid Sediment 15N project) | Used with with a ThermoFinnigan Delta Plus XP isotope ratio mass spectrometer (Thermo Fisher Scientific)
| Trace GC, interfaced via a ConFlo III and GCC device |
Porewater geochemistry data for sediment samples that were included in the global seep survey conducted via Alvin dives from R/V Atlantis cruise AT15-40 in the Guaymas Basin in 2008 | The stable isotopic composition of methane and DIC was determined by GC/C/IRMS using a Hewlett Packard 5890 GC coupled to a Finnegan Mat 252 Isotope Ratio Mass Spectrometer (Hewlett Packard, Wilmington, DE, USA).
| Gas Chromatograph |
Sulfide data for sediment samples that were included in global seep survey from R/V Atlantis cruise AT15-40 and Alvin Dives in the Guaymas Basin in 2008 (Guaymas Basin Vents project, Guaymas Basin interactions project) | The stable isotopic composition of methane and DIC was determined by GC/C/IRMS using a Hewlett Packard 5890 GC coupled to a Finnegan Mat 252 Isotope Ratio Mass Spectrometer (Hewlett Packard, Wilmington, DE, USA).
| Gas Chromatograph |
Porewater geochemistry, including methane, CO2, sulfate, and sulfide from Guaymas Basin hydrothermal sediments collected on R/V Atlantis cruise AT15-56 in Nov-Dec 2009 | Headspace methane concentrations were determined onboard by standard gas chromatography with a flame ionization detector (FID).
| HACH Carle Series 100 AGC Gas Chromatograph |
Sediment geochemistry from push cores collected during HOV Alvin dives during the R/V Atlantis cruise AT37-06 in Guaymas Basin, Gulf of California in December 2016 | DIC was measured with Shimadzu Instruments GC-2014 Gas Chromatograph with FID Detector and Methanizer.
| Shimadzu Instruments GC-2014 |
Sediment geochemistry from push cores collected during HOV Alvin dives during the R/V Atlantis cruise AT37-06 in Guaymas Basin, Gulf of California in December 2016 | Methanol and Ethanol were measured with: a purge and trap system connected to an SRI Instruments 8610C Gas Chromatograph with FID Detector.
| SRI Instruments 8610C |
Sediment geochemistry summary from push cores collected during HOV Alvin dives during the R/V Atlantis cruise AT37-06 in the Guaymas Basin from December 2016 | | Shimadzu Instruments GC-2014 Gas Chromatograph with FID Detector and Methanizer |
Sediment geochemistry summary from push cores collected during HOV Alvin dives during the R/V Atlantis cruise AT37-06 in the Guaymas Basin from December 2016 | | SRI Instruments 8610C Gas Chromatograph with FID Detector |
Sediment geochemistry from push cores collected during HOV Alvin dives during the R/V Atlantis cruise AT42-05 in Guaymas Basin, Gulf of California (27 00.00 N, -111 20.00 W) in November 2018 | | Shimadzu Instruments GC-2014 Gas Chromatograph with FID Detector and Methanizer |
Sediment geochemistry from push cores collected during HOV Alvin dives during the R/V Atlantis cruise AT42-05 in Guaymas Basin, Gulf of California (27 00.00 N, -111 20.00 W) in November 2018 | | SRI Instruments 8610C Gas Chromatograph with FID Detector |
Geochemical measurements of CTD and Alvin Niskin samples collected in the Gulf of California on RV/Atlantis AT42-05 Alvin dives, Nov. 2018 | | SRI Instruments 8610C Gas Chromatograph with FID Detector |
Mean d15N of individual amino acids and bulk organic matter for five plankton size fractions | Used with MAT 253 isotope ratio mass spectrometer (IRMS) via a GC-III combustion (C) interface (Thermo-Finnigan Corporation)
| Thermo Trace GOLD GC |
SF6 and helium data from a tracer release experiment conducted June 2018 in the coastal Baltic Sea during FS Alkor cruise AL510 | Gases stripped from seawater were sent to a molecular sieve column, where SF6 was separated from other gases and then measured with a gas chromatography-electron capture detector (Shimazu GC-14A GC-ECD).
| GC-ECD (Shimazu GC-14A gas chromatography-electron capture detector) |
Cytosolic metallome data of the metalloproteome of Pseudoalteromonas sp. strain BB2-AT2 cultures originally collected from Scripps Pier, California coast in 1995 | Michrom BioResources, Inc. HPLC system containing a Tosoh Bioscience 5-µm particle size TSKgel G3000SWxl size exclusion column with a guard column.
| Tosoh Bioscience 5-µm particle size TSKgel G3000SWxl size exclusion column |
Metalloproteome protein data of the metalloproteome of Pseudoalteromonas sp. strain BB2-AT2 cultures originally collected from Scripps Pier, California coast in 1995 | Michrom BioResources, Inc. HPLC system containing a Tosoh Bioscience 5-µm particle size TSKgel G3000SWxl size exclusion column with a guard column.
| Tosoh Bioscience 5-µm particle size TSKgel G3000SWxl size exclusion column |
Biogeochemistry and microbiology from the R/V Hermano Gines cruises in the Cariaco Basin from 1995 to 2015 (CARIACO Ocean Time-Series Program) | CH4 is assayed by gas chromatography using the vial equilibration technique of Johnson et al. (1990) and a Carle 211AC gas chromatograph.
| Carle 211AC gas chromatograph |
Compound-specific Carbon isotopes from sperm whale dentin from the UC-Santa Cruz labs of P. Koch and M. McCarthy (Sperm Whale SI Ratios project) | Thermo Trace gas chromatograph coupled to a Thermo Finnigan DeltaPlus XP isotope ratio mass spectrometer.
| |
Compound-specific Nitrogen isotopes from sperm whale dentin from the UC-Santa Cruz labs of P. Koch and M. McCarthy (Sperm Whale SI Ratios project) | Thermo Trace gas chromatograph coupled to a Thermo Finnigan DeltaPlus XP isotope ratio mass spectrometer
| |
Bulk and CSIA-AA stable isotopes in sinking POM (sediment trap collected) and proteinaceous deep-sea coral skeletal material in Monterey Bay from 1998 to 2007 | CSIA-AA δ13CAA and δ15NAA values were determined using a gas chromatography (GC) coupled with a Finnigan MAT DeltaPlus XL IRMS at UCSC SIL.
| Thermo Trace Ultra |
Bulk raw isotopic data from tissue samples from pelagic fish from R/V Kilo Moana cruise KM1123 in the north and west of the island of O'ahu in 2011 | Individual amino acids were measured using an IRMS (Delta PlusXP, Delta V Plus or MAT 253) interfaced with a gas chromatograph (Trace GC).
| gas chromatograph |
Barataria Bay carbon mineralization and biogeochemical properties from nine soil cores | Headspace samples were taken at 1, 2, 4, 7, 10, and 14 day time points, and injected into a GC-2014 gas chromatograph (Shimadzu Instrument, Kyoto, Japan) equipped with a flame ionization detector.
| GC-2014 gas chromatograph |
Biogeochemical data on cryptic methane cycling in hypersaline sediments of the Carpinteria Salt Marsh Reserve, California | | Shimadzu GC-2014 |
Nitrous oxide concentrations from CTD bottle samples collected during R/V Hugh R. Sharp cruises HRS1316 and HRS1317 in Chesapeake Bay from August to September of 2013 | Shimadzu GC-14B Gas Chromatograph (GC) equipped with a Porapak-Q packed column and an electron capture detector (ECD)
| Shimadzu GC-14B Gas Chromatograph |
Closed Oyster Mesocosm 15N Tracer (Oyster Reef N2O Emission project) | N2O was measured on a Agilent 7890B GC with a Poropak Column.
| Agilent 7890B GC with a Poropak Column |
Compound specific isotope data of amino acids for abyssal macrofauna, megafauna, sediments, sediment traps, and in situ filtered particles at Station ALOHA off Hawaii and Station M off California from 2019 to 2020 | TFA derivatives of amino acids were analyzed for stable N isotopic composition using a Thermo Scientific Delta V Plus IRMS interfaced to a trace gas chromatograph (GC) fitted with a 60 m BPx5 forte capillary column (0.32 mm internal diameter with 1.0 mm film thickness) through a GC–C III combustion furnace (980 ºC), reduction furnace (680 ºC), and liquid nitrogen cold trap.
| trace gas chromatograph (GC) |
Concentrations of phospholipid-linked fatty acids (PLFAs) in the surface sediments of three marsh ponds in PIE-LTER (Rowley, MA) from 2014. | Used to analyze samples
| Agilent 7890 gas chromatograph |
Physiological measurements during Cyanobacteria Crocosphaera iron/warming experiments | Gas chromatograph GC-8a (Shimadzu Scientific Instruments, Columbia, Maryland),
| Gas chromatograph GC-8a (Shimadzu Scientific Instruments, Columbia, Maryland), |
CSIA-AA comparison between live polyps and outer proteinaceous skeletal material in three taxons of North Pacific deep-sea corals | Compound-specific stable isotopes of amino acids (CSI-AA):
For AA δ13C analyses, the derivatized AAs were injected in split mode at 250°C and separated on a DB-5 column (50 m x 0.5 mm inner diameter; 0.25 mm film thickness; Agilent Technologies, Santa Clara, California, USA) in a Thermo Trace Ultra gas chromatograph (GC) at the University of California, Santa Cruz. The separated AA peaks were analyzed on a Finnegan MAT DeltaPlus XL IRMS interfaced to the GC through a GC-C III combustion furnace (960°C) and reduction furnace (630°C). For AA δ15N analyses, the derivatized AAs were injected in splitless mode at 250 °C and separated on a BPX5 column (60 m x 0.32 mm inner diameter, 1.0 mm film thickness; SGE Analytical Science, Austin, Texas, USA) in the same CG-C-IRMS interfaced through a combustion furnace (980°C), reduction furnace (650°C), and a liquid nitrogen trap.
| Thermo Trace Ultra gas chromatograph (GC) |
N isotopic composition of Phenylalanine and Glutamic Acid from a number of organisms, demonstrating new HPLC protocol for precise isotopic measurements | Isotopic analysis was conducted on a Thermo Trace GC Ultra (Thermo Fisher Scientific, West Palm Beach, FL, USA) coupled via a Thermo GC IsoLink to a ThermoFinnigan DeltaPlus XP isotope ratio monitoring mass spectrometer (Thermo Fisher Scientific).
| Thermo Trace GC Ultra |
N isotopic composition of Phenylalanine and Glutamic Acid from a number of organisms, demonstrating new HPLC protocol for precise isotopic measurements | Derivatives (1 L) were injected (injector temp. 250 degrees C constant) onto an Agilent DB-5 column.
| Agilent DB-5 column |
Results from experiment examining 15N-labeled contaminants in commercial 15N2 gas: Detected 15N-labeled nitrate (NO3) in commercial 15N2 gas (15N2 Contamination project) | The N and O isotopic composition of N2O was then measured on a Delta V Advantage Isotope Ratio Mass Spectrometer (IRMS) interfaced with a modified Gas Bench II gas chromatograph (Thermo Fisher) purge and trap system.
| Gas Chromatograph |
Size and chemical responses of two dinoflagellate species used in natural high light exposure experiments (Protist Signaling project) | Used to analyze samples and standards
| Shimadzu Gas Chromatograph |
Results from experiment examining 15N-labeled contaminants in commercial 15N2 gas: 46-N2O contamination measured directly in commercial 15N2 gas (15N2 Contamination project) | The N and O isotopic composition of N2O was then measured on a Delta V Advantage Isotope Ratio Mass Spectrometer (IRMS) interfaced with a modified Gas Bench II gas chromatograph (Thermo Fisher) purge and trap system.
| Gas Chromatograph |
Discrete O2 Argon (Ar) from NOAA Ship Ronald H. Brown cruise RB-08-02 in the Southwest Atlantic sector of the Southern Ocean near South Georgia Island in 2008 (SO_GasEx project) | Others are chromatographed to separate O2 and Ar from N2
| Gas Chromatograph |
Dimethylsulfide (DMS) and Dymethylsulfonoiproprionate (DMSP) from phyto and microzooplankton experiments from the RVIB Nathaniel B. Palmer NBP0601 cruise in the Ross Sea, Southern Ocean from 2005-2006(CORSACS project, Antarctic microzooplankton project) | A cryogenic purge and trap systems coupled to either a Hewlett-Packard 5890 Series II gas chromatograph and an Agilent 6890 gas chromatograph that were fitted with flame photometric detectors (DiTullio and Smith, 1995) were used to determine DMS and DMSP.
| Gas Chromatograph |
DOM analysis by liquid chromatography 21T fourier transform ion cyclotron resonance mass spectrometry with filtered seawater collected during a Bermuda Atlantic Time Series cruise AE1912 aboard R/V Atlantic Explorer in June of 2019 | Samples were analyzed by 21 Tesla Fourier Transform Ion Cyclotron Resonance Mass Spectrometer coupled to a microflow high pressure chromatography system (Ultimate 3000 RSLCnano, Thermo Scientific). The 21 T FT-ICR MS was designed and built in the Environmental Molecular Sciences Laboratory at the Pacific Northwest National Laboratory 26. The ESIMS was equipped with a heated electrospray ionization source set to a capillary voltage of 3200 V, sheath, auxiliary, and sweep gas flow rates of 15, 3, and 1 (arbitrary units), ion transfer tube temperature of 300°C, vaporizer temperature of 75°C. Mass spectra were collected with 1.5 second transients with a maximum ion accumulation time of 250 ms in positive ionization mode.
| Ultimate 3000 RSLCnano |
Experimental results: Chlorophyll-a, POC, and cell volume of E. huxleyi at 3 pCO2 levels, 2011-2012 (E Hux Response to pCO2 project) | Shimadzu GC-14A gas chromatograph
| Gas Chromatograph |
Carbon and nitrogen content of E. huxleyi at 3 pCO2 levels, 2011-2012 (E Hux Response to pCO2 project) | Shimadzu GC-14A gas chromatograph
| Gas Chromatograph |
Experimental results: Emiliania huxleyi growth rates under different pCO2 levels from Bellingham, WA from 2011-2012 (E Hux Response to pCO2 project) | Shimadzu GC-14A gas chromatograph
| Gas Chromatograph |
Experimental results: cellular particulate DMSP from E. huxleyi at 3 pCO2 levels, 2011-2012 (E Hux Response to pCO2 project) | Shimadzu GC-14A gas chromatograph
| Gas Chromatograph |
Experimental results: Emiliania huxleyi growth rates under different pCO2 levels, 2011-2012 (E Hux Response to pCO2 project) | Shimadzu GC-14A gas chromatograph
| Gas Chromatograph |
Cell size and chemical characteristics of five strains of coccolithophore Emiliania huxleyi (Protist signaling project) | Used to measure Dimethylsulfoniopropionate (DMSP)
| Shimadzu GC-14A gas chromatograph |
MPn-derived methane production by epiphytic bacteria on pelagic Sargassum seaweed from 2017-2019 (Cyanobacteria Hydrocarbons project) | Headspace sampling was performed in small batches to minimize disruption of incubations and methane concentrations were measured via Shimadzu GC-FID 8A with N2 as the carrier gas (Kinnaman et al., 2007). A 3 mL headspace volume was taken from each bottle by syringe and injected into the GC-FID’s gas injection manifold. The syringe was purged three times with N2 gas before headspace sample collection and between each following measurement. Data was recorded with a Shimadzu C-R68A, and the instrument was calibrated with a 3-point calibration curve at the beginning of each sampling period.
| Shimadzu GC-FID 8A |
Dimethylsulfoniopropionate (DMSP) concentrations and turnover during a deployment of the Environmental Sample Processor in Fall, 2014 in Monterey Bay, CA | To measure DMSP concentrations
| Shimadzu GC-2014 gas chromatograph equipped with a Chromosil 330 column and a flame photometric detector for quantification |
Fatty acid data from infauna in sediment cores at McMurdo Station, Antarctica in September, November and February of 2012 and 2013 (McMurdo Benthos project) | Isotopic analysis was measured on a Thermo 1310 gas chromatograph with a Flame Ionization detector using a TR-WaxMS column (30mx 0.32mm x 0.25 um).
| Thermo 1310 gas chromatograph |
Fatty acid measurements for animals used in laboratory-based experiments collected from the Gulf of Mexico Estuary near Port Aransas, Texas from 2020 to 2022 | | Shimadzu GC-2014 gas chromatograph with a flame ionization detector |
Fatty acid measurements for various marine samples collected from the Gulf of Mexico Estuary near Port Aransas, Texas from 2020 to 2022 as well as of red drum eggs spawned from captive adults from 2020 to 2022 | | Shimadzu GC-2014 gas chromatograph with a flame ionization detector |
Fatty acid profiles of M. menidia females and their unfertilized eggs. | Used to quantify fatty acids
| Shimadzu GC-2014 gas chromatograph set with a Phenomenex ZB-WAX plus capillary column |
Geochemical measurements of porewater from sediment push core samples in the Gulf of California during R/V Falkor cruise FK190211 in 2019 | | SRI Instruments 8610C Gas Chromatograph with FID Detector |
Geochemical measurements of porewater from sediment push core samples in the Gulf of California during R/V Falkor cruise FK190211 in 2019 | | Shimadzu Instruments GC-2014 Gas Chromatograph with FID Detector and Methanizer |
Geochemical measurements of CTD and Alvin Niskin samples collected in the Gulf of California during R/V Falkor cruise FK190211 in 2019 | | Shimadzu Instruments GC-2014 Gas Chromatograph with FID Detector and Methanizer |
Geochemical measurements of CTD and Alvin Niskin samples collected in the Gulf of California during R/V Falkor cruise FK190211 in 2019 | | SRI Instruments 8610C Gas Chromatograph with FID Detector |
Summary geochemistry and radiotracer rates for 30 marine sediment cores covering eight sites and four geochemical regimes | SRI 8610C gas chromatograph with flame ionization detector (FID), 1.8m x 3.17 mm Hayecep D packed column, helium carrier, calibrated with certified gas standards (Scotty Specialty Gases; 0.01% UHP CH4 in helium balance).
| gas chromatography |
Concentrations of CFC-11, CFC-12, CFC-113 and SF6 in seawater from the GEOTRACES-Arctic program, aboard RV/HLY-1502, 2015. | Dual ECD (electron capture detector) HP6890 gas chromatograph
| |
CFC-12, CFC-11, and SF6 concentrations from the US GEOTRACES Pacific Meridional Transect (PMT) cruise (GP15) from September to November 2018 | | custom-built purge and trap gas chromatography with electron capture detection |
CFC-12, CFC-11, CFC-113, and SF6 concentration from US GEOTRACES EPZT cruise (R/V Thomas G. Thompson TN303) in the Eastern Tropical Pacific from October to December 2013 | | |
Particulate Acid-Volatile Sulfide (pAVS) and elemental selenium (pSe) concentrations from a McLane pump collected during the R/V Thomas G. Thompson cruise TN303 from Peru to Tahiti in 2013 (U.S. GEOTRACES EPZT project) | Gas chromatograph/flame photometric ionizer
| Gas chromatograph |
Arsenate, iodide, and selenium concentrations collected from Go-FLO bottles during the R/V Thomas G. Thompson cruise TN303 from Peru to Tahiti in 2013 (U.S. GEOTRACES EPZT project) | Processing description says it was used as described in the following reference.
Cutter, L.S., G.A. Cutter, and M.L.C. San Diego‑McGlone. 1991. Simultaneous determination of inorganic arsenic and antimony species in natural waters using selective hydride generation with gas chromatography/photoionization detection. Anal. Chem. 63:1138‑1142. http://dx.doi.org/10.1021%2Fac00011a015
| gas chromatography/photoionization detector |
Growth rates, bulk isotope values, elemental composition data from the R/V Meteor M77 cruise in the Peruvian ocean margin from November to December 2008. | Used with MAT 253 isotope ratio mass spectrometer (IRMS) via a GC-III combustion (C) interface (Thermo-Finnigan Corporation)
| Thermo Trace GOLD GC |
Surface arsenic, antimony speciation, and alkaline phosphatase activity along with US GEOTRACES North Atlantic Transect from the R/V Knorr KN199-04, KN199-05 cruises in the subtropical N. Atlantic during 2010 (U.S. GEOTRACES NAT project) | (tbd)
| Gas Chromatograph |
Depth profiles of seawater d18O and dD from R/V Knorr KN199-04 in the subtropical N. Atlantic Ocean from Oct. 2010 (U.S. GEOTRACES NAT project, GEOTRACES: Intercal Phosphate Oxygen project) | PoraPlot Q GC column, 25m x 0.32mm, Varian, at 50C).
| Gas Chromatograph |
Concentrations of CFC-11, CFC-12, CFC-113 and SF6 in seawater from R/V Knorr KN199-04 (GT10), KN204-01 (GT11) in the subtropical northern Atlantic Ocean from 2010-2011 (U.S. GEOTRACES NAT project) |
Dual ECD (electron capture detector) HP6890 gas chromatograph
| Gas Chromatograph |
Surface transects for arsenic speciation, antimony speciation, and alkaline phosphatase activity from R/V Knorr cruise KN204-01 in the Subtropical North Atlantic Ocean in 2011 (U.S. GEOTRACES NAT project) | | Gas Chromatograph |
Depth profiles for arsenic and antimony speciation and alkaline phosphatase activity from R/V Knorr cruise KN204-01 in the Subtropical North Atlantic Ocean in 2011 (U.S. GEOTRACES NAT project) | | Gas Chromatograph |
Porewater methane concentrations from sediment cores collected on the Guaymas Basin Ridge flanks and the Sonora Margin in 2014 from R/V El Puma in October 2014 | Methane isotopic composition was measured by gas chromatography coupled with mass spectrometry (Chanton and Liptay 2014).
| gas chromatography |
Porewater methane concentrations and d13C-CH4 values in Alvin pushcore samples from Guaymas Basin hydrothermal sediments collected on R/V Atlantis cruise AT37-06 in December 2016 | Methane samples were analyzed by headspace gas chromatography-flame ionization detection (GC-FID).
| |
Halomethane concentrations in San Pedro Ocean Time series (SPOT) from March to December 2017 | Agilent 7890A Gas Chromatograph with electron capture detector. Column- Restek Rtx-502.2 (60m, 0.32mm ID, 1.8µm)
| Agilent 7890A Gas Chromatograph |
Halomethane concentrations in cell culture | Column- Restek Rtx-502.2 (60m, 0.32mm ID, 1.8µm df)
| Agilent 7890A Gas Chromatograph with electron capture detector |
Radiocarbon DIC, DIC concentration, pH, and [CH4] in Hudson Canyon, northern US Atlantic Margin collected from R/V Endeavor cruise EN541 in July 2014 | | Agilent 6850 gas chromatograph |
Hydrocarbon compounds identified and measured in sediments and porewaters using gas chromatography from R/V JOIDES Resolution IODP-385 cruise in the Guaymas Basin between September and November, 2019. | All hydrocarbon analyses were performed with Gas Chromatography at Alpha Analytical Labs, Mansfiled MA.
| Gas Chromatography |
Porewater hydrocarbon concentrations in Alvin pushcore samples from Guaymas Basin hydrothermal vents, RV/Atlantis cruise AT42-05, Nov. 2018 | | |
Sediment hydrocarbon concentrations in Alvin pushcore samples from Guaymas Basin hydrothermal vents, RV/Atlantis cruise AT42-05, Nov. 2018 | | |
Vascular plant and microbial biomarkers of dissolved organic matter data from incubation experiments | Lignin phenol monomers were measured as trimethylsilane derivatives using an Agilent 6890N GC/5975 MS.
| Agilent 6890N GC/5975 MS |
Supplementary Table 2: Drill fluid contamination testiFMC in drilling. GC mass spectrometry measurements of concentrations of the tracers PFMD and Png fluid and sample materials | | Gas Chromatograph (GC) Hewlett Packard 5890 |
Isotopes in methane in natural waters of Alaska | CH4 concentrations for all samples were measured on an SRI 310 Gas Chromatograph (GC) equipped with a flame ionization detector and an Alltech Haysep S 100/120 column (6’ x 1/8” x 0.085”).
| SRI 310 Gas Chromatograph (GC) |
Isotopic composition of phospholipid-linked fatty acids (PLFAs) in the surface sediments of three marsh ponds in PIE-LTER (Rowley, MA) from 2014. | Used to analyze samples
| Agilent 7890 gas chromatograph |
Isotopic composition of phospholipid-linked fatty acids (PLFAs) in the surface sediments of three marsh ponds in PIE-LTER (Rowley, MA) from 2014. | Used to determine stable carbon isotope ratios of FAMEs
| Hewlett-Packard 6890 GC |
Concentrations of DMS, DMSPp, DMSPd, & DMSOd in relation to ocean acidification [H+] during the KOSMOS 2014 mesocosm experiment off Gran Canaria | Procedures for the analysis of reduced sulfur compounds was based on purge-and-cryotrap approaches linked to a gas chromatograph with either flame FPD or mass spectrometric detector.
| gas chromatograph |
Lake Michigan water chemistry data, including dissolved and particulate phosphorus, chlorophyll a, carbon dioxide, total dissolved inorganic carbon, and dissolved organic carbon from 2017 to 2020 | SRI 8610C Gas chromatograph. This instrument was used to measured the CO2 and DIC concentration in water samples. The instrument was calibrated against CO2 standards with an accuracy of +/- 3%.
| SRI 8610C Gas chromatograph |
Methane concentrations (depths of 5-175 m) at Station ALOHA collected during Hawaii Ocean Time-Series cruises between 2008 and 2016 (HOT project) | | gas chromatograph (GC) Agilent 7890A |
Methane and sulfate concentration profiles - sediment cores from White Oak River estuary in October 2012 (IODP-347 Microbial Quantification project) | Agilent 7890a gas chromatograph equipped with flame ionization detector
| |
Microbial diversity and geochemistry of marine sediment mesocosm, Cape Lookout Bight, North Carolina | gas chromatograph with a flame ionized detector (Agilent, Santa Clara, CA)
| |
Amino acid compound specific isotope values for micronekton from R/V Kilo Moana KM1109, KM1123, KM1407, KM1418, and other cruises in the Central North Pacific, Station ALOHA, Tropical Pacific, 2007-2014 | | Thermo Finnigan GC-C III |
Modern deep-sea coral (Desmophyllum dianthus) nitrogen isotopes from samples collected between 1961 and 2009 (DeepSeaCoralNitrogen project) | | Gas chromatography |
N isotopic composition of Phenylalanine and Glutamic Acid from a number of organisms, demonstrating new HPLC protocol for precise isotopic measurements | Isotopic analysis was conducted on a Thermo Trace GC Ultra (Thermo Fisher Scientific, West Palm Beach, FL, USA) coupled via a Thermo GC IsoLink to a ThermoFinnigan DeltaPlus XP isotope ratio monitoring mass spectrometer (Thermo Fisher Scientific).
| Thermo Trace GC Ultra |
N isotopic composition of Phenylalanine and Glutamic Acid from a number of organisms, demonstrating new HPLC protocol for precise isotopic measurements | Derivatives (1 L) were injected (injector temp. 250 degrees C constant) onto an Agilent DB-5 column.
| Agilent DB-5 column |
N and O isotope effects of nitrate reduction by 3 forms of nitrate reductase (15N2 Contamination project) | NO3- δ15N and δ18O were determined with the denitrifier method (Sigman et al. 2001; Casciotti et al. 2002), wherein denitrifying bacteria lacking terminal nitrous oxide reductase (P. chlororaphis f. sp. aureofaciens ATCC 1398) quantitatively convert sample NO3- to N2O gas, which is then extracted, purified and analyzed through a modified Thermo-Scientific Gas Bench II and Delta V Advantage gas chromatograph isotope ratio mass spectrometer.
| gas chromatograph |
Results from experiment examining 15N-labeled contaminants in commercial 15N2 gas: The measured quantity of 15N2 added to nitrate and ammonium solutions equilibrated with 15N2 gas | The N and O isotopic composition of N2O was then measured on a Delta V Advantage Isotope Ratio Mass Spectrometer (IRMS) interfaced with a modified Gas Bench II gas chromatograph (Thermo Fisher) purge and trap system.
To measure the d15N of N2 gas in the headspace of experimental samples, 75 uL of headspace was injected into 12 mL Exetainer vials previously flushed with helium, then analyzed on a Gas Bench II GC-IRMS (Delta V Advantage Plus) operated in continuous flow mode.
| Gas Chromatograph |
Dissolved N2O and aquatic nutrient concentrations from 4 field sites in Bogue Sound, North Carolina collected from 2014 to 2015. | Used to analyze N2O
| Gas Chromatograph |
Global reconstruction of surface oceanic N2O disequilibrium and its associated flux | GOSHIP: Shipboard gas chromatography-electron capture detection (GC-ECD)
SPOT: SRI 8610 Greenhouse Gas Monitoring Gas Chromatograph (GC) equipped with an electron capture detector (ECD), dual HayeSep D packed columns, and a 1-mL sample loop (SRI Instruments, Torrance, California, USA).
| Shipboard gas chromatography-electron capture detection |
Environmental data from Niskin bottle sampling during the Fall 2016 ESP deployment in Monterey Bay, CA | | Shimadzu GC-2014 gas chromatograph |
Nitrogen and carbon fixation rates and POC and PON from thermal variation experiment of Trichodesmium GBR strain from 2016-2018 | Used to measure Nitrogen fixation rates
| Shimadzu gas chromatograph GC-8a (Shimadzu Scientific Instruments) |
15N2-based N2 fixation rates from the Eastern Tropical South Pacific collected on the R/V Atlantis (AT15-61) and R/V Melville (MV1104) in 2010-2011 (N2 fixation ETSP project) | | Gas Chromatograph |
N2O concentrations from San Pedro Ocean Time-series (SPOT) measured between 2014 to 2016 | | SRI Greenhouse Gas Monitoring Gas Chromatograph |
Nitrous oxide concentrations (depths of 5-175 m) at Station ALOHA collected during Hawaii Ocean Time-Series cruises between 2008 and 2016 (HOT project) | For quantifying the dissolved gases, the analytical column (30 m x 0.32 mm GS-CarbonPLOT capillary column; J&W Scientific) was housed within a gas chromatograph (GC) Agilent 7890A equipped with a flame ionization detector (FID) and an electron capture detector (ECD). The carrier flow was alternated from the FID to the ECD using a Dean’s switch® (Agilent Technologies) which allowed the quantification of both CH4 and N2O from a single sample.
| gas chromatograph (GC) Agilent 7890A |
Carbonate chemistry analyses of water collected from near Walpole, ME from zooplankton hatching experiments during 2011 | A Shimadzu Model GC-6A gas chromatograph (gc) with a thermal conductivity detector was used to determine concentrations of total carbon dioxide (TCO2).
| Gas Chromatograph |
Open Mesocosm Oyster 15N2 and N2O | N2O was measured on a Agilent 7890B GC with a Poropak Column.
| Agilent 7890B GC with a Poropak Column |
Standing stocks and rates for organic sulfur compounds during summer in the subarctic Northeast Pacific | | Shimadzu GC2014-with Flame Photometric Detector |
Other solutes from vertical profiles from multi- and gravity cores from two cruises, R/V Robert Gordon Sproul SP1215 and R/V New Horizon NH1319, in the Santa Barbara and Santa Monica Basins in 2012 and 2013 | | |
Amino acid compound specific isotope values for particles from R/V Kilo Moana KM1407 and KM1418 in the Central North Pacific, Station ALOHA, Tropical Pacific, Feb and Sept. 2014 | Used to analyze amino acids.
| Thermo Scientific Delta V Plus IRMS |
Particle d15N values of amino acids from EXPORTS cruises SR1812 on R/V Sally Ride and RR1813 on R/V Roger Revelle in August to September 2018 | | Thermo Fisher Scientific Trace 1310 Gas Chromatograph |
| A Thermo Delta V gas chromatograph isotope ratio mass spectrometer (GC-IRMS) - used to analyze N isotopes of nitrous oxide gas derived from the chemical oxidation of NH4+ using the hypobromite-azide method (Zhang et al. 2007), with calibrations achieved using NH4+ reference materials IAEA-N1 and IAEA-N2.
| Thermo Delta V gas chromatograph isotope ratio mass spectrometer (GC-IRMS) |
Biogeochemical and sediment characteristics of the Cinder Cones Methane seep site in the Ross Sea from November 2016 | Methane concentration was measured with a HP 5890 Gas Chromatograph with an AllTech Porapak N8/100 column and a Flame ionization detector.
| HP 5890 Gas Chromatograph |
Porewater geochemistry (sulfate, methane, and DIC) from sediments of the White Oak River (WOR), NC, Station H in 2013 (SEDpep project) | Headspace methane was measured by gas chromatography.
| gas chromatograph |
Porewater geochemistry data for sediment samples included in global seep survey from R/V Atlantis cruise AT15-40 and Alvin dives in the Guaymas Basin in 2008 (Guaymas Basin interactions project) | Stable isotopic values and concentrations of DIC were analyzed via coupled GC (Hewlett Packard 5890) and Isotope Ratio Mass Spectrometer (Finnigan MAT 252).
| Hewlett Packard 5890 |
Stable carbon isotope data for thirteen individual amino acids from twelve species of eukaryotic microalgae and four species of eukaryotic microalgae | Thermo Trace 1310 gas chromatograph (GC) and analyzed on a Finnegan MAT Delta V Plus Isotope Ratio Mass Spectrometer (IRMS) interfaced to the GC through a GC-IsoLink II and reduction furnace (1000°C) used to separate and analyze the carbon isotope values of 13 individual amino acids from each sample and standard.
| Thermo Trace 1310 gas chromatograph (GC) |
Nitrous oxide concentrations from the R/V Falkor expedition FK160115 in the Central Pacific from January to February 2016 | Nitrous oxide concentration: N2O concentrations were measured using a headspace equilibration method and analyzed on a SRI Greenhouse Gas Monitoring Gas Chromatograph (GC) equipped with an electron capture detector (ECD), dual HayeSep D packed columns, and a 1-mL sample loop (SRI Instruments, Torrance, California, USA; Elkins 1980; Laperriere et al. 2019).
| RI Greenhouse Gas Monitoring Gas Chromatograph |
Radiocarbon in methane from waters of the US Atlantic and Pacific margins as collected on R/V Hugh Sharp cruise HRS1713 and R/V Rachel Carson cruise RC0026 in 2017 and 2019 | Methane concentration measurements were performed in the Kessler laboratory at the University of Rochester using an Agilent 6850 gas chromatograph with a flame ionization detector (GC-FID).
| Agilent 6850 GC-FID |
Compound-specific carbon isotopes from sperm whale skin tissue from the UC-Santa Cruz labs of P. Koch and M. McCarthy (Sperm Whale SI Ratios project) | | |
Sperm whale skin tissue samples analyzed for C and N at UC-Santa Cruz: date and location of collection from the California Current System | | |
Vascular plant and microbial biomarkers of dissolved organic matter from San Francisco Bay transects | Lignin phenol monomers were measured as trimethylsilane derivatives using an Agilent 6890N GC/5975 MS.
| Agilent 6890N GC/5975 MS |
Hydrocarbon concentrations, DIC isotopes, nutrients, and cyanobacteria counts from samples collected on R/V Neil Armstrong cruise AR16 in the western north Atlantic during May 2017 | | gas chromatograph flame ionization detector (GC-FID) |
N2O, 15N2, 15N tissue tracer in oyster aquariums (Oyster Reef N2O Emission project) | N2O was measured on a Agilent 7890B GC with a Poropak Column.
| Agilent 7890B GC with a Poropak Column |
Fatty acid signature profiles of harbor seals and prey species determined by flame ionization detection (FID) for samples collected in the San Juan Islands of Washington State in 2007-2008 (Seal_response_to_prey project) | Samples were separated on a Hewlett-Packard 5890 gas chromatograph with flame ionization detector (Hewlett-Packard Co., Palo Alto, CA).
| Gas Chromatograph |
Sediment delta-13C methane and concentrations from pushcore samples collected at Guaymas Basin hydrothermal vents via Alvin dives on RV/Atlantis cruise AT42-05, Nov. 2018 | Used to measure carbon isotopes (Agilent) and to measure methane concentrations (HP 5890)
| Agilent 6890 gas chromatograph and an Hewlett Packard 5890 gas chromatograph with an FID detector |
Raw concentrations of individual PLFA compounds from Massachusetts from 2012-2015. | Analyzed samples
| Agilent 7890 gas chromatograph |
Sediment PLFA isotope values from Massachusetts collected from 2012-2015 | effluent split ~70:30
| Agilent 7890 gas chromatograph |
Shotgun Proteomics of Bering Sea algal incubations. | | Agilent 6890 capillary GC |
Compound-specific isotope analysis of amino acids (CSIA-AA) from a subset of siphophore samples collected during four research cruises on the R/V Wester Flyer in the California Current Ecosystem between 2019 and 2021 | Derivatives were analyzed using a Thermo-Finnigan Delta V Plus isotope ratio mass spectrometer (IRMS), interfaced with a Thermo Trace GC gas chromatograph via GC-C III combustion furnace (980°C), reduction furnace (680°C), and a liquid nitrogen cold trap.
| Thermo Trace GC gas chromatograph |
Southern Ocean deep-sea fossil coral (Desmophyllum dianthus) nitrogen isotope records generated using Monte Carlo and Kalman Filters generated using Monte Carlo and Kalman Filters (DeepSeaCoralNitrogen project) | | Gas chromatography |
Southern Ocean deep-sea fossil coral (Desmophyllum dianthus) nitrogen isotopes from R/V Nathaniel B. Palmer and R/V Thompson cruises between 2008 and 2011 (DeepSeaCoralNitrogen project) | | Gas chromatography |
Spring 2011 -Sediment Gas Concentrations and Stable Isotope Values | Stable isotope data were obtained from a gas chromatograph coupled to as stable isotope ratio monitoring mass spectrometer
| Gas Chromatograph |
Cell abundance, nutrient and DMSP concentrations measured during a mesocosm study of the effect of phytoplankton composition on bacterial DMSP transformation (OceanSulfurFluxBact project) | To measure DMSP concentrations
| Shimadzu GC-2014 gas chromatograph equipped with a Chromosil 330 column and a flame photometric detector for quantification |
Record of abundance and δ2H of dinosterol in down core lake sediments from T Lake, Palau collected in September 2013 | 6890N GC (Agilent). Gas chromatograph equipped with flame ionization detector and PTV (programmable temperature volatilization) inlet.
| 6890N GC (Agilent) |
Record of abundance and δ2H of dinosterol in down core lake sediments from T Lake, Palau collected in September 2013 | Trace GC Ultra (Thermo). Gas chromatograph equipped with pyrolysis interface (GC-TC II) and split/splitless inlet.
| Trace GC Ultra (Thermo) |
Fatty acid profiles by biovolume of replicate populations of Thalassiosira pseudonana, selected at 16 and 31C for ~500 generations and assayed at 4 temperatures | Gas chromatograph using the Agilent capillary DB‐23 column for FAME analysis. Temperature settings: initial temperature 140°C, increased by 30°C/min to 160°C, then by 8°C/min to 240°C, and held at 240°C for 2 min.
| Agilent Technologies 7890A Gas Chromatography system (Agilent Technologies) |
Fatty acid profiles per cell of replicate populations of Thalassiosira pseudonana, selected at 16 and 31C for ~500 generations and assayed at 4 temperatures | Gas chromatograph using the Agilent capillary DB‐23 column for FAME analysis. Temperature settings: initial temperature 140°C, increased by 30°C/min to 160°C, then by 8°C/min to 240°C, and held at 240°C for 2 min.
| Agilent Technologies 7890A Gas Chromatography system (Agilent Technologies) |
Table 2: Carbonate data and nutrients measured during Calanus finmarchicus and Meganyctiphanes norvegica egg hatching success experiments, 2011-2012 | Used to measure Total CO2, determined by acid stripping a 1.113 ml volume of water sample or TCO2 standard, trapping the expelled CO2, and then injecting it into the chromatograph had a thermal conductivity detector.
| Shimadzu Model GC-8A gas chromatograph |
The influence of reactive oxygen species on "‘respiration" isotope effect | | 3 m gas chromatography (GC) column |
Trichodesmium nutrient-limited proteomes in 380 and 750 uatm CO2 from experiments conducted at the University of Southern California from 2011-2013 (HiCO2_AdaptCyano project) | Shimadzu Scientific Instruments, Columbia, Maryland. Equipped with a flame ionization detector.
| Shimadzu gas chromatograph GC-8a |
Experimental results from a study of CO2 and N2 fixation and trichome length of Trichodesmium erythraeum under varying pCO2 and light conditions (PhytoTM_in_HighCO2 project) | Gas chromatograph model: GC-8A, Shimadzu Scientific Instruments, Columbia, MD, USA used in determination of N2 fixation.
| Gas Chromatograph |
Triple oxygen isotopes of respiration and photo-oxidation of DOC | Oxygen gas was separated from N2 and Ar using a 3 m gas chromatography (GC) column.
| gas chromatography |
Water column analytical data from the Chile Triple Junction collected on two cruises aboard the R/V Melville during February-March 2010 and April 2012 | | SRI 8610C gas chromatograph |
Concentration measurements of water column phosphate, nitrate and nitrite, dissolved organic phosphorus, methane, and ethylene from samples collected during the R/V Neil Armstrong cruise AR16 in the western North Atlantic Ocean in May 2017 | | Agilent 7980A |
Water column radiotracer methane oxidation rates in the Guaymas Basin, Gulf of California from R/V Atlantis cruise AT42-05 in 2018 and R/V Falkor cruise FK190211 in 2019 | | SRI Instruments 8610C Gas Chromatograph with FID Detector |
Compound specific isotopic analysis (15N) of the amino acids of size-fractionated zooplankton collected near the Chatham Rise on the R/V Tangaroa SalpPOOP (TAN1810) cruise in Oct. and Nov. of 2018 | Thermo Trace GC 1310 gas chromatograph coupled to a Thermo Scientific Delta V Advantage isotope-ratio mass spectrometer via a GC IsoLink II combustion interface.
| Thermo Trace GC 1310 gas chromatograph |
Size fractionated zooplankton d13C and d15N of individual amino acids from EXPORTS cruise RR1813 in August 2018 | CSIA-AA was carried out on a gas chromatograph coupled to an isotope ratio mass spectrometer (GC-IRMS).
| gas chromatograph |
CSIA 15N AA data from phytoplankton, microzooplankton, and Calanus pacificus. | Used with mass spectrometer
| Trace GC gas chromatograph, GC 1310 gas chromatograph |
CSIA 15N AA data from phytoplankton, microzooplankton, and Calanus pacificus. | Coupled to a GC Isolink combustion-reduction furnace (1000 deg C) and liquid nitrogen cold trap.
| GC 1310 |